Swagelok2E002 is a hardware fixture developed by the SCI Materials Hub for two-electrode battery testing, with an electrode area of Φ 6mm - Φ 20mm (standard size Φ 14mm), and can be customized according to the users' needs. The Swagelok2E002 battery test hardware allows you to easily conduct electrochemical experiments. Moreover, its compactness and ergonomic design allows users to easily use it in the glovebox, and ensures perfect air tightness and repeatability of experiments.
Users can select materials of the reaction chamber and conductive metal cylinders according to the experimental requirements.
The polymer reaction chamber is resistant to highly aggressive solvents, has high resistance, and ensures excellent durability over time.
The metal reaction chamber has high conductivity. Different from the polymer reaction chamber, when the metal reaction chamber is used to assemble the battery, a layer of polyester film (such as Mylar film) is required to provide an electrical insulation layer between the reaction chamber and the electrode/conductive metal cylinders.
| Battery test type | Battery Components (standard electrode area Φ14mm) | Details |
| Swagelok2E002-1 normal battery test | Conductive copper pillar (x2), 316L conductive cylinder (x1), 316L conductive cylinder with hump (x1), 316L conductive spacer with hump (x1) PP nut (x2), PTFE sealing ring (x2), 304L stainless steel spring (x1), PP reaction chamber (x1), DC electrical lead pair with crocodile clip to O-ring connector (x2), 304 screws (x2) | The operating temperature range is - 30~120 °C. It is generally recommended that the long-term operating temperature should not be higher than 100 °C, USD$80/set |
| Swagelok2E002-2 normal battery test (Pressurizable type) | Conductive copper pillar (x2), 316L conductive cylinder (x2), PP nut (x2), PTFE sealing ring (x2) PP reaction chamber (x1), DC electrical lead pair with crocodile clip to O-ring connector (x2), 304 screws (x2) | The operating temperature range is - 30~120 °C. It is generally recommended that the long-term operating temperature should not be higher than 100 °C, $ 80/set |
| Swagelok2E002-3 medium-high temperature battery test | Conductive copper pillar (x2), 316L conductive cylinder (x1), 316L conductive cylinder with hump (x1), 316L conductive spacer with hump (x1) PTFE nut (x2), PTFE sealing ring (x2), 304L stainless steel spring (x1), PTFE reaction chamber (x1) DC electrical lead pair with crocodile clip to O-ring connector (x2), 304 screws (x2) | It is made of high temperature resistant PTFE, and the operating temperature range is - 180~260 °C. $100/set |
| Swagelok2E002-4 medium-high temperature battery test (Pressurizable type) | Conductive copper pillar (x2), 316L conductive cylinder (x2), PTFE nut (x2), PTFE seal ring (x2) PTFE reaction chamber (x1), DC electrical lead pair with crocodile clip to O-ring connector (x2), 304 screws (x2) | It is made of high temperature resistant PTFE, and the operating temperature range is - 180~260 °C. $100/set |
| Swagelok2E002-5 High temperature battery test | Conductive copper pillar (x2), 316L conductive cylinder (x1), 316L conductive cylinder with hump (x1), 316L conductive spacer with hump (x1) PEEK nut (x2), PEEK seal ring (x2), 304L stainless steel spring (x1), PEEK reaction chamber (x1) DC electrical lead pair with crocodile clip to O-ring connector (x2), 304 screws (x2) | It is made of high temperature resistant PEEK material, and the operating temperature range is - 40~300 °C. The maximum instantaneous operating temperature can reach 310 °C, $120/set |
| Swagelok2E002-6 High temperature battery test (Pressurizable type) | Conductive copper pillar (x2), 316L conductive cylinder (x2), PEEK nut (x2), PEEK seal ring (x2) PEEK reaction chamber (x1), DC electrical lead pair with crocodile clip to O-ring connector (x2), 304 screws (x2) | High temperature resistant PEEK material is used. The operating temperature range is - 40~300 °C. The maximum instantaneous operating temperature can reach 310 °C. $120/set |
| Swagelok2E002-7 Observable battery test | Conductive copper pillar (x2), 316L conductive cylinder (x1), 316L conductive cylinder with hump (x1), 316L conductive spacer with hump (x1) PP nut (x2), PTFE sealing ring (x2), 304L stainless steel spring (x1), acrylic reaction chamber (x1) DC electrical lead pair with crocodile clip to O-ring connector (x2), 304 screws (x2) | Transparent acrylic material is used, and the operating temperature range is not higher than 60 °C. $100/set |
| Swagelok2E002-8 Observable battery test (Pressurizable type) | Conductive copper pillar (x2), 316L conductive cylinder (x2), PP nut (x2), PTFE sealing ring (x2) Acrylic reaction chamber (x1), DC electrical lead pair with crocodile clip to O-ring connector (x2), 304 screws (x2) | Transparent acrylic material is used, and the operating temperature range is not higher than 60 °C. $100/set |
| Swagelok2E002-9 Normal corrosion resistance battery test 1 | Conductive copper pillar (x2), titanium conductive cylinder (x1), titanium conductive cylinder with hump (x1), titanium conductive spacer with hump (x1), PP nut (x2) PTFE sealing ring (x2), titanium spring (x1), PP reaction chamber (x1) DC electrical lead pair with crocodile clip to O-ring connector (x2), 304 screws (x2) | The service temperature range is - 30~120 °C. It is generally recommended that the long-term service temperature should not be higher than 100 °C. $160/set |
| Swagelok2E002-10 Normal corrosion resistance battery test 2 (Pressurizable type) | Conductive copper pillar (x2), titanium conductive cylinder (x2), PP nut (x2), PTFE sealing ring (x2) PP reaction chamber (x1), DC electrical lead pair with crocodile clip to O-ring connector (x2), 304 screws (x2) | The operating temperature range is - 30~120 °C. It is generally recommended that the long-term operating temperature should not be higher than 100 °C. $160/set |
| Swagelok2E002-11 Normal corrosion resistance battery test 3 | Conductive copper pillar (x2), molybdenum conductive cylinder (x1), molybdenum conductive cylinder with hump (x1), molybdenum conductive spacer with hump (x1), PP nut (x2) PTFE sealing ring (x2), titanium spring (x1), PP reaction chamber (x1) DC electrical lead pair with crocodile clip to O-ring connector (x2), 304 screws (x2) | The operating temperature range is - 30~120 °C. It is generally recommended that the long-term operating temperature should not be higher than 100 °C, $200/set |
| Swagelok2E002-12 Normal Corrosion Resistant Battery Test 4 (Pressurizable type) | Conductive copper pillar (x2), molybdenum conductive cylinder (x2), PP nut (x2), PTFE sealing ring (x2), PP reaction chamber (x1), DC electrical lead pair with crocodile clip to O-ring connector (x2), 304 screws (x2) | The operating temperature range is - 30~120 °C. It is generally recommended that the long-term operating temperature should not be higher than 100 °C. $200/set |
| Swagelok2E002-13 Medium-high temperature corrosion resistant battery test 1 | Conductive copper pillar (x2), titanium conductive cylinder (x1), titanium conductive cylinder with hump (x1), titanium conductive spacer with hump (x1), PTFE nut (x2) PTFE sealing ring (x2), titanium spring (x1), PTFE reaction chamber (x1) DC electrical lead pair with crocodile clip to O-ring connector (x2), 304 screws (x2) | It is made of high temperature resistant PTFE, and the operating temperature range is - 180~260 °C $180/set |
| Swagelok2E002-14 Medium-high temperature corrosion resistant battery test 2 (Pressurizable type) | Conductive copper pillar (x2), titanium conductive cylinder (x2), PTFE nut (x2), PTFE sealing ring (x2), PTFE reaction chamber (x1), DC electrical lead pair with crocodile clip to O-ring connector (x2), 304 screws (x2) | It is made of high temperature resistant PTFE, and the operating temperature range is - 180~260 °C. $180/set |
| Swagelok2E002-15 Medium-high temperature corrosion resistant battery test 3 | Conductive copper pillar (x2), molybdenum conductive cylinder (x1), molybdenum conductive cylinder with hump (x1), molybdenum conductive spacer with hump (x1), PTFE nut (x2) PTFE sealing ring (x2), titanium spring (x1), PTFE reaction chamber (x1) DC electrical lead pair with crocodile clip to O-ring connector (x2), 304 screws (x2) | It is made of high temperature resistant PTFE, and the operating temperature range is - 180~260 °C. $220/set |
| Swagelok2E002-16 Medium-high temperature corrosion resistant battery test 4 (Pressurizable type) | Conductive copper pillar (x2), molybdenum conductive cylinder (x2), PTFE nut (x2), PTFE sealing ring (x2), PTFE reaction chamber (x1), DC electrical lead pair with crocodile clip to O-ring connector (x2), 304 screws (x2) | It is made of high temperature resistant PTFE, and the operating temperature range is - 180~260 °C. $220/set |
| Swagelok2E002-17 High temperature corrosion resistant battery test 1 | Conductive copper pillar (x2), titanium conductive cylinder (x1), titanium conductive cylinder with hump (x1), titanium conductive spacer with hump (x1), PEEK nut (x2) PEEK sealing ring (x2), titanium spring (x1), PEEK reaction chamber (x1) DC electrical lead pair with crocodile clip to O-ring connector (x2), 304 screws (x2) | It is made of high temperature resistant PEEK material, and the operating temperature range is - 40~300 °C. The maximum instantaneous operating temperature can reach 310 °C, $200/set |
| Swagelok2E002-18 High temperature corrosion resistant battery test 2 (Pressurizable type) | Conductive copper pillar (x2), titanium conductive cylinder (x2), PEEK nut (x2), PEEK seal ring (x2) PEEK reaction chamber (x1), DC electrical lead pair with crocodile clip to O-ring connector (x2), 304 screws (x2) | It is made of high temperature resistant PEEK material. The operating temperature range is - 40~300 °C, and the maximum instantaneous operating temperature can reach 310 °C. $200/set |
| Swagelok2E002-19 High temperature corrosion resistant battery test 3 | Conductive copper pillar (x2), molybdenum conductive cylinder (x1), molybdenum conductive cylinder with hump (x1), molybdenum conductive spacer with hump (x1), PEEK nut (x2) PEEK sealing ring (x2), titanium spring (x1), PEEK reaction chamber (x1) DC electrical lead pair with crocodile clip to O-ring connector (x2), 304 screws (x2) | It is made of high temperature resistant PEEK material. The operating temperature range is - 40~300 °C, and the maximum instantaneous operating temperature can reach 310 °C. $240/set |
| Swagelok2E002-20 High temperature corrosion resistant battery test 4 (Pressurizable type) | Conductive copper pillar (x2), molybdenum conductive cylinder (x2), PEEK nut (x2), PEEK seal ring (x2), PEEK reaction chamber (x1), DC electrical lead pair with crocodile clip to O-ring connector (x2), 304 screws (x2) | High temperature resistant PEEK material is used. The operating temperature range is - 40~300 °C. The maximum instantaneous operating temperature can reach 310 °C. $240/set |
| Swagelok2E002-21 Observable corrosion resistance battery test 1 | Conductive copper pillar (x2), titanium conductive cylinder (x1), titanium conductive cylinder with hump (x1), titanium conductive spacer with hump (x1), PP nut (x2) PTFE sealing ring (x2), titanium spring (x1), acrylic reaction chamber (x1) DC electrical lead pair with crocodile clip to O-ring connector (x2), 304 screws (x2) | Transparent acrylic material is used, and the operating temperature range is not higher than 60 °C. $180/set |
| Swagelok2E002-22 Observable corrosion resistance battery test 2 (Pressurizable type) | Conductive copper pillar (x2), titanium conductive cylinder (x2), PP nut (x2), PTFE sealing ring (x2), Acrylic reaction chamber (x1), DC electrical lead pair with crocodile clip to O-ring connector (x2), 304 screws (x2) | Transparent acrylic material is used, and the operating temperature range is not higher than 60 °C. $180/set |
| Swagelok2E002-23 Observable corrosion resistance battery test 3 | Conductive copper pillar (x2), molybdenum conductive cylinder (x1), molybdenum conductive cylinder with hump (x1), molybdenum conductive spacer with hump (x1), PP nut (x2) PTFE sealing ring (x2), titanium spring (x1), acrylic reaction chamber (x1) DC electrical lead pair with crocodile clip to O-ring connector (x2), 304 screws (x2) | Transparent acrylic material is used, and the operating temperature range is not higher than 60 °C. $220/set |
| Swagelok2E002-24 Observable corrosion resistance battery test 4 (Pressurizable type) | Conductive copper pillar (x2), molybdenum conductive cylinder (x2), PP nut (x2), PTFE sealing ring (x2), Acrylic reaction chamber (x1), DC electrical lead pair with crocodile clip to O-ring connector (x2), 304 screws (x2) | Transparent acrylic material is used, and the operating temperature range is not higher than 60 °C. $220/set |
| Customized | Reaction chamber: PTFE, PP, acrylic, PEEK, HDPE, PET, PFA, PC, etc Electrode: 316L stainless steel, 904L stainless steel, titanium, molybdenum, etc Electrode area: 6mm-20mm, etc | |
| Optional accessories (standard electrode area 14mm) | |
| Spring | 304L spring ($6/5 pieces), 316L spring ($10/5 pieces), titanium spring ($20/5 pieces) |
| Reaction chamber | PP ($40/piece), acrylic ($50/piece), HDPE ($50/piece), PTFE ($50/piece), PEEK ($60/piece), PFA ($80/piece) |
| Sealing ring | PTFE ($10/piece), PEEK ($10/piece), 316L ($10/piece), titanium ($10/piece) |
Conductive cylinder set with hump | 1 set (including 3 pieces: Conductive cylinder with hump+conductive cylinder+conductive spacer with hump): 316L - $40, 904L - $120, titanium (grade 2) - $120, molybdenum - $160 |
Pressurized conductive cylinder set | 1 set (including 2 conductive cylinder): 316L - $40, 904L - $120, titanium (grade 2) - $120, molybdenum - $160 |
| Other | DC electrical lead pair with crocodile clip to O-ring connector ($4/1 pair), Conductive copper pillar ($ 4/6 pieces), screw ($4/6 pieces) |
Typical Structure of Swagelok2E002 Battery Test Hardware (Two Electrode)
| Accessories | Accessory details | |||
| Reaction chamber | PP（$40/pcs） | PTFE ($50/pcs) | PEEK ($60/pcs) | Acrylic ($50/pcs) |
Boss conductive column 1 set contains 3 pieces: Conductive column + boss conductive column + boss conductive gasket | 316L ($40/set) | Ti ($120/set) | Mo($160/set) | 904L ($120/set) |
Nut 1 set contains 2 pieces |
PP ($16/pcs) |
PTFE ($18/pcs) | PEEKPTFE ($20/pcs) | |
Sealing rings 1 set contains 2 pieces | PTFE | PEEK | ||
| Spring | 316L stainless steel spring | titanium spring | ||
| Other |
Alligator clip conductive wire ($8/2 pair) | screw ($4/6pcs) | Conductive end posts | |
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Partial references citing our materials (from Google Scholar)
Carbon Dioxide Reduction
1. ACS Nano Strain Relaxation in Metal Alloy Catalysts Steers the Product Selectivity of Electrocatalytic CO2 Reduction
The bipolar membrane (Fumasep FBM) in this paper was purchased from SCI Materials Hub, which was used in rechargeable Zn-CO2 battery tests. The authors reported a strain relaxation strategy to determine lattice strains in bimetal MNi alloys (M = Pd, Ag, and Au) and realized an outstanding CO2-to-CO Faradaic efficiency of 96.6% with outstanding activity and durability toward a Zn-CO2 battery.
2. Front. Chem. Boosting Electrochemical Carbon Dioxide Reduction on Atomically Dispersed Nickel Catalyst
In this paper, Vulcan XC-72R was purchased from SCI Materials Hub. Vulcan XC 72R carbon is the most common catalyst support used in the anode and cathode electrodes of Polymer Electrolyte Membrane Fuel Cells (PEMFC), Direct Methanol Fuel Cells (DMFC), Alkaline Fuel Cells (AFC), Microbial Fuel Cells (MFC), Phosphoric Acid Fuel Cells (PAFC), and many more!
3. Adv. Mater. Partially Nitrided Ni Nanoclusters Achieve Energy-Efficient Electrocatalytic CO2 Reduction to CO at Ultralow Overpotential
An AEM membrane (Sustainion X37-50 Grade RT, purchased from SCI Materials Hub) was activated in 1 M KOH for 24 h, washed with ultra-purity water prior to use.
4. Adv. Funct. Mater. Nanoconfined Molecular Catalysts in Integrated Gas Diffusion Electrodes for High-Current-Density CO2 Electroreduction
In this paper (Supporting Information), an anion exchanged membrane (Fumasep FAB-PK-130 obtained from SCI Materials Hub (www.scimaterials.cn)) was used to separate the catholyte and anolyte chambers.
SCI Materials Hub: we also recommend our Fumasep FAB-PK-75 for the use in a flow cell.
5. Appl. Catal. B Efficient utilization of nickel single atoms for CO2 electroreduction by constructing 3D interconnected nitrogen-doped carbon tube network
In this paper, the Nafion 117 membrane was obtained from SCI Materials Hub.
In this paper, Proton exchange membrane (Nafion 117), Nafion D520, and Toray 060 carbon paper were purchased from SCI Materials Hub.
7. National Science Review Confinement of ionomer for electrocatalytic CO2 reduction reaction via efficient mass transfer pathways
An anion exchange membrane (PiperION-A15-HCO3) was obtained from SCI Materials Hub.
8. Catalysis Communications Facilitating CO2 electroreduction to C2H4 through facile regulating {100} & {111} grain boundary of Cu2O
Carbon paper (TGPH060), membrane solution (Nafion D520), and ionic membrane (Nafion N117) were obtained from Wuhu Eryi Material Technology Co., Ltd (a company under SCI Materials Hub).
Batteries
1. J. Mater. Chem. A Blocking polysulfides with a Janus Fe3C/N-CNF@RGO electrode via physiochemical confinement and catalytic conversion for high-performance lithium–sulfur batteries
Graphene oxide (GO) in this paper was obtained from SCI Materials Hub. The authors introduced a Janus Fe3C/N-CNF@RGO electrode consisting of 1D Fe3C decorated N-doped carbon nanofibers (Fe3C/N-CNFs) side and 2D reduced graphene oxide (RGO) side as the free-standing carrier of Li2S6 catholyte to improve the overall electrochemical performance of Li-S batteries.
This paper used more than 10 kinds of materials from SCI Materials Hub and the authors gave detailed properity comparsion.
The commercial IEMs of Fumasep FAB-PK-130 and Nafion N117 were obtained from SCI Materials Hub.
Gas diffusion layers of GDL340 (CeTech) and SGL39BC (Sigracet) and Nafion dispersion (Nafion D520) were obtained from SCI Materials Hub.
Zn foil (100 mm thickness) and Zn powder were obtained from the SCI Materials Hub.
Commercial 20% Pt/C, 40% Pt/C and IrO2 catalysts were also obtained from SCI Materials Hub.
3. Journal of Energy Chemistry Vanadium oxide nanospheres encapsulated in N-doped carbon nanofibers with morphology and defect dual-engineering toward advanced aqueous zinc-ion batteries
In this paper, carbon cloth (W0S1011) was obtained from SCI Materials Hub. The flexible carbon cloth matrix guaranteed the stabilization of the electrode and improved the conductivity of the cathode.
4. Energy Storage Materials Defect-abundant commercializable 3D carbon papers for fabricating composite Li anode with high loading and long life
The 3D carbon paper (TGPH060 raw paper) were purchased from SCI Materials Hub.
5. Nanomaterials A Stable Rechargeable Aqueous Zn–Air Battery Enabled by Heterogeneous MoS2 Cathode Catalysts
Nafion D520 (5 wt%), and carbon paper (GDL340) were received from SCI-Materials-Hub.
Carbon cloth (W0S1011) and other electrochemical consumables required for air cathode were provided by SCI Materials Hub.
Oxygen Reduction Reaction
1. J. Chem. Eng. Superior Efficiency Hydrogen Peroxide Production in Acidic Media through Epoxy Group Adjacent to Co-O/C Active Centers on Carbon Black
In this paper, Vulcan XC 72 carbon black, ion membrane (Nafion N115, 127 μL), Nafion solution (D520, 5 wt%), and carbon paper (AvCarb GDS 2230 and Spectracarb 2050A-1050) were purchased from SCI Materials Hub.
2. Journal of Colloid and Interface Science Gaining insight into the impact of electronic property and interface electrostatic field on ORR kinetics in alloy engineering via theoretical prognostication and experimental validation
The 20 wt% Pt3M (M = Cr, Co, Cu, Pd, Sn, and Ir) were purchased from SCI Materials Hub. This work places emphasis on the kinetics of the ORR concerning Pt3M (M = Cr, Co, Cu, Pd, Sn, and Ir) catalysts, and integrates theoretical prognostication and experimental validation to illuminate the fundamental principles of alloy engineering.
Water Electrolysis
1. International Journal of Hydrogen Energy Gold as an efficient hydrogen isotope separation catalyst in proton exchange membrane water electrolysis
The cathodic catalysts of Pt/C (20 wt%, 2–3 nm) and Au/C (20 wt%, 4–5 nm) were purchased from SCI Materials Hub.
2. Small Science Silver Compositing Boosts Water Electrolysis Activity and Durability of RuO2 in a Proton-Exchange-Membrane Water Electrolyzer
Two fiber felts (0.35 mm thickness, SCI Materials Hub) were used as the porous transport layers at both the cathode and the anode.
3. Advanced Functional Materials Hierarchical Crystalline/Amorphous Heterostructure MoNi/NiMoOx for Electrochemical Hydrogen Evolution with Industry-Level Activity and Stability
Anion-exchange membrane (FAA-3-PK-130) was obtained from SCI Materials Hub website.
Fuel Cells
1. Polymer Sub-two-micron ultrathin proton exchange membrane with reinforced mechanical strength
Gas diffusion electrode (60% Pt/C, Carbon paper) was purchased from SCI Materials Hub.
Characterization
1. Chemical Engineering Journal Electrochemical reconstitution of Prussian blue analogue for coupling furfural electro-oxidation with photo-assisted hydrogen evolution reaction
An Au nanoparticle film was deposited on the total reflecting plane of a single reflection ATR crystal (SCI Materials Hub, Wuhu, China) via sputter coater.
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