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EmStat4R Mini electrochemistry analyzer

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  • Description:EmStat4R Mini electrochemistry analyzer
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The EmStat4R delivers desktop performance in a rugged enclosure. The EmStat4R is a portable Battery or USB-powered Potentiostat, Galvanostat, and optional a Frequency Response Analyzer (FRA) for Electrochemical Impedance Spectroscopy (EIS). The EmStat4R is great for applications that require low currents, from 30 mA down to picoamps, such as sensor applications. The EmStat4R is controlled with PSTrace for Windows, the Android app PStouch, or you can write your own MethodSCRIPT and control it from any platform or operating system. The EmStat4R is available with a cell cable or SPE connection module. Both versions can be configured with optional EIS/FRA with a maximum frequency of 200 kHz.


Supported Techniques
Voltammetric techniques
Linear Sweep VoltammetryLSV
Cyclic VoltammetryCV
Fast Cyclic VoltammetryFCV
AC VoltammetryACV
Pulsed techniques
Differential Pulse VoltammetryDPV
Square Wave VoltammetrySWV
Normal Pulse VoltammetryNPV
Amperometric techniques
ChronoamperometryCA
Zero Resistance AmperometryZRA
ChronocoulometryCC
MultiStep AmperometryMA
Fast AmperometryFAM
Pulsed Amperometric DetectionPAD
Multiple-Pulse Amperometric DetectionMPAD
Calvanostatic techniques
Linear Sweep PotentiometryLSP
ChronopotentiometryCP
MultiStep PotentiometryMP
Open Circuit PotentiometryOCP
Stripping ChronopotentiometrySCP or PSA
Potentiostatic/Galvanostatic Impedance spectroscopy (EIS/GEIS)
Potential scan or current scan
Fixed potential or fixed current
Time scan
Other
Mixed ModeMM


System Specifications
General
dc-potential range±3V
compliance voltage±5V
maximum current±30mA
max.cata acquisition rate1M samples/s
Potentiostat (controlled potential mode)
appliec potential resolution100uV
applied potential accuracy≤0.2% ±1mV offset
current ranges1nA to 10mA
measured current resolution0.009% of CR (92fA on 1nA range)
measured current accuracy<0.2% of current, ±20pA ±0.2% of range
bandwidth settings320Hz, 3.2kHz, 30kHz, 570kHz
Galvanostat (controlled current mode)
current ranges10nA, 1uA, 100uA, 10mA, 4 ranges
applied dc-current±3*CR (current range)
applied dc-current resolution0.01% of CR
applied dc-current accuracy<0.4% of current, ±20 pA ±0.2% of range
potential ranges50mV, 100mV, 200mv, 500mv, 1V
measured dc-potential resolution96 uV(1V),
48uV(500mV),
19.2uV(200mV),
9.6uV(100mV),
4.8uV(50mV)
measured dc-potential accuracy≤0.2% potential, 1 mV offset
bandwidth settings320Hz, 3.2kHz, 30kHz or 570kHz
FRA / EIS (impedance measurements)
frequenoy range10uHz to 200kHz
ac-amplitude range1mV to 900mV rms, or 2.5V p-p
GEIS (galvanostatic impedance measurements)
frequency range10uHz to 200kHz
ac-amplitude range0.9*CR A rms
Electrometer
electrometer amplifier input> 1TΩ // 10pF
bandwidth10kHz or 500kHz
Other
housingaluminum body only: 11.1 x 6.0 x 2.7 cm
with rubber sleeve: 11.8 x 6.8 x 3.3 cm
weight~ 310 g
powerUSB-C port
communicationUSB-C or Bluetooth
battery life>6 hours with cell on at 10 mA current
charging up to 80% takes approx. 3.5 hours
a full charge takes approx. 5 hours
internal storage space500MB, equivalent to >15M datapoints


Measurement Specifications
ParameterMinMax
All techniques(unless otherwise specified)Conditioning time04000s
Deposition time04000s
Equilibration time04000s
Step potential0.100mV250mV
N data points31,000,000
NPVScan rate0.1mV/s (100uV step)1V/s (5mV step)
DPVPulse time0.4ms300ms
SWVFrequency1Hz2500Hz
LSV
CV
Scan rate0.01mV/s (100uV step)500V/s (200mV step)
PADlnterval time50ms300s
Pulse time1ms1s
N data points31000000(100 days at 10 sinterval)
CA CP OCPlnterval time0.4ms300s
Run time1ms>year
MM MA MPN cycles120000
N levels1255
lnterval time50ms300S


EmStat4R SNSEmStat4R SPE
Connection moduleCell cableConnection moduleScreen-printed-electrode
Cell cable includedYesCell cable includedNo
Electrode connectionsWE, RE, CE and groundElectrode connectionsRE, WE, CE
Connectors2mm banana plugsSensor pitch2.54mm
FRA/EIS (Yes/No)10uHz to 200kHzMaximum sensor width11mm
Product image

Allowed sensor thicknessBetween 0.1mm and 0.8mm
FRA/EIS (Yes/No)10uHz to 200kHz
Product image


Standard EmStat4R Kit
1、a rugged carrying case
2、EmStat4R instrument with SNS Connection Module (for use with 1 m cell cable)
or SPE Connection Module (for use with Screen Printed Electrodes)
3、USB-C cable
4、1 meter cell cable with 2 mm banana pins
5、Optional additional SNS or SPE Connection Module
6、PSTrace software for Windows (on USB drive
7、Manual (hardcopy)
8、Quick Start document
9、Calibration report
Product image


For internaltional orders, please ask us for quotes via

Email: contact@scimaterials.cn

Tel: +86 15375698751

Wechat: SCI-Materials-Hub


Article code:
Price(USD)
ES4R-SNS.F0EmStat4R SNS with no EIS4920
ES4R-SNS.F1EmStat4R SNS with EIS5920
ES4R-SPE.F0EmStat4R SPE with no EIS4700
ES4R-SPE.F1EmStat4R SPE with EIS5700

Remark:
F0 means no EIS.
F1 means having EIS.


Worldwide shipping via DHL, SF-Express & other requested carriers.

Payments via Bank Transfer, Paypal, Credit card (via Alibaba), Alipay, Wechat-pay are accepted.


Partial references citing our materials (from Google Scholar)


Carbon Dioxide Reduction

1. ACS Nano Strain Relaxation in Metal Alloy Catalysts Steers the Product Selectivity of Electrocatalytic CO2 Reduction

The bipolar membrane (Fumasep FBM) in this paper was purchased from SCI Materials Hub, which was used in rechargeable Zn-CO2 battery tests. The authors reported a strain relaxation strategy to determine lattice strains in bimetal MNi alloys (M = Pd, Ag, and Au) and realized an outstanding CO2-to-CO Faradaic efficiency of 96.6% with outstanding activity and durability toward a Zn-CO2 battery.


2. Front. Chem. Boosting Electrochemical Carbon Dioxide Reduction on Atomically Dispersed Nickel Catalyst

In this paper, Vulcan XC-72R was purchased from SCI Materials Hub. Vulcan XC 72R carbon is the most common catalyst support used in the anode and cathode electrodes of Polymer Electrolyte Membrane Fuel Cells (PEMFC), Direct Methanol Fuel Cells (DMFC), Alkaline Fuel Cells (AFC), Microbial Fuel Cells (MFC), Phosphoric Acid Fuel Cells (PAFC), and many more!


3. Adv. Mater. Partially Nitrided Ni Nanoclusters Achieve Energy-Efficient Electrocatalytic CO2 Reduction to CO at Ultralow Overpotential

An AEM membrane (Sustainion X37-50 Grade RT, purchased from SCI Materials Hub) was activated in 1 M KOH for 24 h, washed with ultra-purity water prior to use.


4. Adv. Funct. Mater. Nanoconfined Molecular Catalysts in Integrated Gas Diffusion Electrodes for High-Current-Density CO2 Electroreduction

In this paper (Supporting Information), an anion exchanged membrane (Fumasep FAB-PK-130 obtained from SCI Materials Hub (www.scimaterials.cn)) was used to separate the catholyte and anolyte chambers.

SCI Materials Hub: we also recommend our Fumasep FAB-PK-75 for the use in a flow cell.


5. Appl. Catal. B Efficient utilization of nickel single atoms for CO2 electroreduction by constructing 3D interconnected nitrogen-doped carbon tube network

In this paper, the Nafion 117 membrane was obtained from SCI Materials Hub.


6. Vacuum Modulable Cu(0)/Cu(I)/Cu(II) sites of Cu/C catalysts derived from MOF for highly selective CO2 electroreduction to hydrocarbons

In this paper, Proton exchange membrane (Nafion 117), Nafion D520, and Toray 060 carbon paper were purchased from SCI Materials Hub.


7. National Science Review Confinement of ionomer for electrocatalytic CO2 reduction reaction via efficient mass transfer pathways

An anion exchange membrane (PiperION-A15-HCO3) was obtained from SCI Materials Hub.


8. Catalysis Communications Facilitating CO2 electroreduction to C2H4 through facile regulating {100} & {111} grain boundary of Cu2O

Carbon paper (TGPH060), membrane solution (Nafion D520), and ionic membrane (Nafion N117) were obtained from Wuhu Eryi Material Technology Co., Ltd (a company under SCI Materials Hub).


Batteries

1. J. Mater. Chem. A Blocking polysulfides with a Janus Fe3C/N-CNF@RGO electrode via physiochemical confinement and catalytic conversion for high-performance lithium–sulfur batteries

Graphene oxide (GO) in this paper was obtained from SCI Materials Hub. The authors introduced a Janus Fe3C/N-CNF@RGO electrode consisting of 1D Fe3C decorated N-doped carbon nanofibers (Fe3C/N-CNFs) side and 2D reduced graphene oxide (RGO) side as the free-standing carrier of Li2S6 catholyte to improve the overall electrochemical performance of Li-S batteries.


2. Joule A high-voltage and stable zinc-air battery enabled by dual-hydrophobic-induced proton shuttle shielding

This paper used more than 10 kinds of materials from SCI Materials Hub and the authors gave detailed properity comparsion.

The commercial IEMs of Fumasep FAB-PK-130 and Nafion N117 were obtained from SCI Materials Hub.

Gas diffusion layers of GDL340 (CeTech) and SGL39BC (Sigracet) and Nafion dispersion (Nafion D520) were obtained from SCI Materials Hub.

Zn foil (100 mm thickness) and Zn powder were obtained from the SCI Materials Hub.

Commercial 20% Pt/C, 40% Pt/C and IrO2 catalysts were also obtained from SCI Materials Hub.


3. Journal of Energy Chemistry Vanadium oxide nanospheres encapsulated in N-doped carbon nanofibers with morphology and defect dual-engineering toward advanced aqueous zinc-ion batteries

In this paper, carbon cloth (W0S1011) was obtained from SCI Materials Hub. The flexible carbon cloth matrix guaranteed the stabilization of the electrode and improved the conductivity of the cathode.


4. Energy Storage Materials Defect-abundant commercializable 3D carbon papers for fabricating composite Li anode with high loading and long life

The 3D carbon paper (TGPH060 raw paper) were purchased from SCI Materials Hub.


5. Nanomaterials A Stable Rechargeable Aqueous Zn–Air Battery Enabled by Heterogeneous MoS2 Cathode Catalysts

Nafion D520 (5 wt%), and carbon paper (GDL340) were received from SCI-Materials-Hub.


6. SSRN An Axially Directed Cobalt-Phthalocyanine Covalent Organic Polymer as High-Efficient Bifunctional Catalyst for Zn-Air Battery

Carbon cloth (W0S1011) and other electrochemical consumables required for air cathode were provided by SCI Materials Hub.


Oxygen Reduction Reaction

1. J. Chem. Eng. Superior Efficiency Hydrogen Peroxide Production in Acidic Media through Epoxy Group Adjacent to Co-O/C Active Centers on Carbon Black

In this paper, Vulcan XC 72 carbon black, ion membrane (Nafion N115, 127 μL), Nafion solution (D520, 5 wt%), and carbon paper (AvCarb GDS 2230 and Spectracarb 2050A-1050) were purchased from SCI Materials Hub.


2. Journal of Colloid and Interface Science Gaining insight into the impact of electronic property and interface electrostatic field on ORR kinetics in alloy engineering via theoretical prognostication and experimental validation

The 20 wt% Pt3M (M = Cr, Co, Cu, Pd, Sn, and Ir) were purchased from SCI Materials Hub. This work places emphasis on the kinetics of the ORR concerning Pt3M (M = Cr, Co, Cu, Pd, Sn, and Ir) catalysts, and integrates theoretical prognostication and experimental validation to illuminate the fundamental principles of alloy engineering.


Water Electrolysis

1. International Journal of Hydrogen Energy Gold as an efficient hydrogen isotope separation catalyst in proton exchange membrane water electrolysis

The cathodic catalysts of Pt/C (20 wt%, 2–3 nm) and Au/C (20 wt%, 4–5 nm) were purchased from SCI Materials Hub.


2. Small Science Silver Compositing Boosts Water Electrolysis Activity and Durability of RuO2 in a Proton-Exchange-Membrane Water Electrolyzer

Two fiber felts (0.35 mm thickness, SCI Materials Hub) were used as the porous transport layers at both the cathode and the anode.


3. Advanced Functional Materials Hierarchical Crystalline/Amorphous Heterostructure MoNi/NiMoOx for Electrochemical Hydrogen Evolution with Industry-Level Activity and Stability

Anion-exchange membrane (FAA-3-PK-130) was obtained from SCI Materials Hub website.


Fuel Cells

1. Polymer Sub-two-micron ultrathin proton exchange membrane with reinforced mechanical strength

Gas diffusion electrode (60% Pt/C, Carbon paper) was purchased from SCI Materials Hub.


Characterization

1. Chemical Engineering Journal Electrochemical reconstitution of Prussian blue analogue for coupling furfural electro-oxidation with photo-assisted hydrogen evolution reaction

An Au nanoparticle film was deposited on the total reflecting plane of a single reflection ATR crystal (SCI Materials Hub, Wuhu, China) via sputter coater.

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